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I'm pretty sure you can use "sobre mi cadáver", which means "over my dead body" or "you'd have to kill me first".
There is a related phrase "primero muerto" which is used as a response meaning "I'd rather be dead".
-- ¿Quieres ser mi novia?
-- Primero muerta.
-- Will you be my girlfriend?
-- I'd rather die than be your girlfriend.
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If you find something wrong with my Spanish, please correct it!
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